N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

Base Information

Chemical Name:N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine
CAS No.:163617-85-4
Molecular Formula:C₂₅H₃₀N₂O₂
Molecular Weight:390.525
Hs Code.:

Synonyms:N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

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Technology Process of N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

There total 1 articles about N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5729-16-8
N-(4-methoxy-benzyl)-benzene-1,2-diamine

: 2094-72-6
1-Adamantanecarbonyl chloride

: 163617-85-4
N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 60 ℃; for 1.5h;
DOI:10.1016/j.bmc.2011.05.057

Reference yield:

: 163617-85-4
N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

: 163617-86-5
N-(1-adamantyl)methyl-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

Guidance literature:: N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine; With dimethylsulfide borane complex; In tetrahydrofuran; at 10 - 110 ℃; for 1.25h; Inert atmosphere;

With methanol; sodium carbonate; for 3h; Reflux;
DOI:10.1016/j.bmc.2011.05.057

Reference yield:

: 163617-85-4
N-(1-adamantanecarbonyl)-N'-(4-methoxyphenyl)methyl-1,2-phenylenediamine

: 163617-90-1
N-[1-(1-adamantyl)methyl-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-3-yl]-N'-phenylurea

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 1.25 h / 10 - 110 °C / Inert atmosphere

1.2: 3 h / Reflux

2.1: ethyl acetate / 2 h / Reflux

3.1: acetic acid; zinc / 0.25 h / 23 °C

3.2: pH 10

4.1: ammonium cerium (IV) nitrate; water / acetonitrile / 36 h / 23 °C

5.1: dichloromethane / 0.5 h / 23 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; dimethylsulfide borane complex; water; acetic acid; zinc; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2011.05.057