2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

Base Information

Chemical Name:2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene
CAS No.:1356140-58-3
Molecular Formula:C₇₆H₁₄₄I₂O₂
Molecular Weight:1343.79
Hs Code.:

Synonyms:2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

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Chemical Property of 2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

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Technology Process of 2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

There total 10 articles about 2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1356140-56-1
1-iodo-11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl]dodecane

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 1356140-58-3
2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h; Inert atmosphere;
DOI:10.1002/asia.201100480

Reference yield:

: 916226-09-0
2,5-bis(methoxymethoxy)-1,4-diiodobenzene

: 1356140-58-3
2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/asia.201100480

Reference yield:

: C₁₈H₃₀O₄

: 1356140-58-3
2,5-bis{11-methyl-7-(4-methylpentyl)-3-[8-methyl-4-(4-methylpentyl)nonyl] dodecyloxy}-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 6 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

2.2: 6 h / 20 °C / 760.05 Torr

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 12 h / 20 °C

4.2: 6 h / 20 °C / 760.05 Torr

5.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 6 h / 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

With 1H-imidazole; triethylsilane; Jones reagent; sulfuric acid; iodine; potassium carbonate; magnesium; triphenylphosphine; trifluoroacetic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; 1.1: Jones oxidation;
DOI:10.1002/asia.201100480