6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

Base Information

Chemical Name:6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide
CAS No.:916250-68-5
Molecular Formula:C₆₁H₇₄ClN₄O₁₀P₃
Molecular Weight:1151.65
Hs Code.:

6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

Synonyms:6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

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Chemical Property of 6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

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Technology Process of 6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

There total 5 articles about 6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 916250-62-9
N-[3-(2-amino-3-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-propoxy)-propyl]-2-(diphenyl-phosphinoyl)-acetamide

: 19347-73-0
6-chlorohexanoyl chloride

: 916250-68-5
6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

Guidance literature:: With potassium carbonate; In dichloromethane; water; at 20 ℃; for 24h;
DOI:10.1039/b600412a

Reference yield:

: 916250-59-4
{2-[3-(2-chloro-acetylamino)-propoxy]-1,1-bis-[3-(2-chloro-acetylamino)-propoxymethyl]-ethyl}-carbamic acid benzyl ester

: 916250-68-5
6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 1 h / 150 °C

2: 87 percent / H₂ / 10 percent Pd/C / methanol

3: 68 percent / K₂CO₃ / CH₂Cl₂; H₂O / 24 h / 20 °C

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; water; 1: Arbuzov reaction;
DOI:10.1039/b600412a

Reference yield:

: 916250-60-7
(2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-carbamic acid benzyl ester

: 916250-68-5
6-chloro-hexanoic acid (2-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxy}-1,1-bis-{3-[2-(diphenyl-phosphinoyl)-acetylamino]-propoxymethyl}-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / H₂ / 10 percent Pd/C / methanol

2: 68 percent / K₂CO₃ / CH₂Cl₂; H₂O / 24 h / 20 °C

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1039/b600412a