22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Base Information

Chemical Name:22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol
CAS No.:133910-17-5
Molecular Formula:C₂₅H₄₂O₂Si
Molecular Weight:402.693
Hs Code.:

Synonyms:22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Suppliers and Price of 22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Chemical Property:

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Technology Process of 22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

There total 4 articles about 22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14452-30-3
3'-iodoacetophenone

: 133910-17-5
22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; diethyl ether / 1 h / 0 °C

2: CH₂Cl₂ / 12 h / 20 °C

In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00112a021

Reference yield:

: 102879-20-9
2-(3-iodophenyl)propan-2-ol

: 133910-17-5
22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 12 h / 20 °C

In dichloromethane;
DOI:10.1021/jm00112a021

Reference yield:

: 618-51-9
3-Iodobenzoic acid

: 133910-17-5
22-<3-<1'-methyl-1'-<(trimethylsilyl)oxy>ethyl>phenyl>-de-A,B-24-norcholan-8β-ol

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; diethyl ether / 2 h / 0 °C

2: tetrahydrofuran; diethyl ether / 1 h / 0 °C

3: CH₂Cl₂ / 12 h / 20 °C

In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00112a021