C₁₉H₁₉BIN₃O

Base Information

Chemical Name:C₁₉H₁₉BIN₃O
CAS No.:1447963-03-2
Molecular Formula:C₁₉H₁₉BIN₃O
Molecular Weight:443.095
Hs Code.:

C<sub>19</sub>H<sub>19</sub>BIN<sub>3</sub>O

Synonyms:C₁₉H₁₉BIN₃O

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Chemical Property of C₁₉H₁₉BIN₃O

Chemical Property:

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Technology Process of C₁₉H₁₉BIN₃O

There total 4 articles about C₁₉H₁₉BIN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447963-02-1
C₂₄H₂₇BIN₃O₃

: 1447963-03-2
C₁₉H₁₉BIN₃O

Guidance literature:: With 2,6-dimethylpyridine; t-butyldimethylsiyl triflate; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.06.043

Reference yield:

: 89694-50-8
(2-iodo-5-methoxyphenyl)boronic acid

: 1447963-03-2
C₁₉H₁₉BIN₃O

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane; n-heptane / 12 h / -78 - 20 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: toluene; dimethyl sulfoxide / 12 h / 120 °C / Inert atmosphere; Dean-Stark

3.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

4.1: t-butyldimethylsiyl triflate; 2,6-dimethylpyridine / dichloromethane / 12 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; t-butyldimethylsiyl triflate; boron tribromide; potassium carbonate; potassium iodide; In n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2013.06.043

Reference yield:

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 1447963-03-2
C₁₉H₁₉BIN₃O

Guidance literature:: Multi-step reaction with 5 steps

1.1: iodine; silver nitrate

2.1: boron tribromide / dichloromethane; n-heptane / 12 h / -78 - 20 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: toluene; dimethyl sulfoxide / 12 h / 120 °C / Inert atmosphere; Dean-Stark

4.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

5.1: t-butyldimethylsiyl triflate; 2,6-dimethylpyridine / dichloromethane / 12 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; t-butyldimethylsiyl triflate; iodine; boron tribromide; potassium carbonate; silver nitrate; potassium iodide; In n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2013.06.043