(2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene

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Chemical Name:(2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene
CAS No.:99232-71-0
Molecular Formula:C₂₅H₂₂O₆
Molecular Weight:418.446
Hs Code.:
Mol file:99232-71-0.mol

Synonyms:(2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene

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Chemical Property of (2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene Edit

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Technology Process of (2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene

There total 2 articles about (2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 96247-02-8
(2R)-trans-2-acetoxy-3-hydroxy-1-[(benzoyloxy)methyl]cyclohexa-4,6-diene

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 99232-71-0
(2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo00225a015

Reference yield:

: 86782-19-6
(2R)-trans-2,3-diacetoxy-1-[(benzoyloxy)methyl]cyclohexa-4,6-diene

: 99232-71-0
(2R)-trans-2-acetoxy-3-<(E)-cinnamoyloxy>-1-<(benzoyloxy)methyl>cyclohexa-4,6-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / p-toluenesulfonic acid / methanol

2: 62 percent / CH₂Cl₂; pyridine / 0.17 h / -50 °C

With toluene-4-sulfonic acid; In pyridine; methanol; dichloromethane;
DOI:10.1246/bcsj.59.655