C₂₉H₄₆N₄O₆S₂

Base Information

• Chemical Name: C₂₉H₄₆N₄O₆S₂
• CAS No.: 1357067-88-9
• Molecular Formula: C₂₉H₄₆N₄O₆S₂
• Molecular Weight: 610.839
• Mol file: 1357067-88-9.mol

Synonyms:C₂₉H₄₆N₄O₆S₂

Chemical Property of C₂₉H₄₆N₄O₆S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₆N₄O₆S₂

There total 6 articles about C₂₉H₄₆N₄O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H48N4O7S2 (1357067-87-8) → C29H46N4O6S2 (1357067-88-9)

Guidance literature:

With lithium hydroxide monohydrate; water; In methanol;

Reference yield:

Boc-Lys-thiazolidide (371241-75-7) → C29H46N4O6S2 (1357067-88-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

2.1: water; lithium hydroxide monohydrate / methanol

3.1: triethylamine; methanesulfonyl chloride / dmap / dichloromethane / 20 °C

3.3: 17 h / 60 °C / Inert atmosphere

4.1: water; lithium hydroxide monohydrate / methanol

With lithium hydroxide monohydrate; water; benzotriazol-1-ol; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; dmap; In methanol; dichloromethane;

Reference yield:

Boc-Lys(pNZ)-OH (22601-53-2) → C29H46N4O6S2 (1357067-88-9)

Guidance literature:

Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

3.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

4.1: water; lithium hydroxide monohydrate / methanol

5.1: triethylamine; methanesulfonyl chloride / dmap / dichloromethane / 20 °C

5.3: 17 h / 60 °C / Inert atmosphere

6.1: water; lithium hydroxide monohydrate / methanol

With lithium hydroxide monohydrate; water; hydrogen; benzotriazol-1-ol; methanesulfonyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; dmap; palladium 10% on activated carbon; In methanol; dichloromethane;

upstream raw materials:

Boc-Lys-thiazolidide

Boc-Lys(pNZ)-OH

C₂₂H₃₂N₄O₇S

C₃₁H₄₈N₄O₈S

Downstream raw materials:

C₁₉H₃₀N₄O₂S₂