dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

Base Information

Chemical Name:dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride
CAS No.:1455481-74-9
Molecular Formula:C₁₈H₂₇F₅NP
Molecular Weight:383.385
Hs Code.:

Synonyms:dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

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Chemical Property of dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

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Technology Process of dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

There total 4 articles about dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1455481-76-1
1,1-difluoro-N,N-dimethyl-1-[4-(4-propylcyclohexyl)phenyl]methanamine

: 1455481-74-9
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

Guidance literature:: With trifluorophosphane; In diethyl ether; at -196 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: trans-4-(4-n-propylcyclohexyl)benzoic acid

: 1455481-74-9
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / Inert atmosphere; Reflux

2.1: Inert atmosphere

3.1: oxalyl dichloride / dichloromethane / Inert atmosphere; Reflux

3.2: 3 h / 20 °C / Inert atmosphere

4.1: trifluorophosphane / diethyl ether / -196 °C / Inert atmosphere

With thionyl chloride; oxalyl dichloride; trifluorophosphane; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 82492-58-8
4-(trans-4'-propylcyclohexyl) benzoic acid chloride

: 1455481-74-9
dimethylamino[4-(4-propylcyclohexyl)phenyl]methylidene-phosphorus(V) pentafluoride

Guidance literature:: Multi-step reaction with 3 steps

1.1: Inert atmosphere

2.1: oxalyl dichloride / dichloromethane / Inert atmosphere; Reflux

2.2: 3 h / 20 °C / Inert atmosphere

3.1: trifluorophosphane / diethyl ether / -196 °C / Inert atmosphere

With oxalyl dichloride; trifluorophosphane; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2013.07.062