Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

Base Information

Chemical Name:Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester
CAS No.:224580-09-0
Molecular Formula:C₂₉H₄₃F₃O₄
Molecular Weight:512.653
Hs Code.:

Synonyms:Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

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Chemical Property of Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

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Technology Process of Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

There total 7 articles about Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 407-25-0
trifluoroacetic anhydride

: 224580-08-9
(6R,7S)-6-(4-Methoxy-benzyloxy)-2,6,7-trimethyl-9-methylene-pentadec-2-en-8-ol

: 224580-09-0
Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(99)00207-5

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 224580-09-0
Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / CSA / CH₂Cl₂

2: 86 percent / DIBAL / CH₂Cl₂

3: NMO, TPAP

4: 1.) t-BuLi

5: 70 percent / Et₃N, DMAP / CH₂Cl₂

With dmap; N-methyl-2-indolinone; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; tert.-butyl lithium; diisobutylaluminium hydride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(99)00207-5

Reference yield:

: 50727-94-1,62777-72-4,62960-04-7,71030-55-2,76985-26-7,82188-73-6,112456-40-3,112456-65-2,62777-71-3
(2R,3R)-3-methyl-3-(4-methyl-3-pentenyl)oxiranemethanol

: 224580-09-0
Trifluoro-acetic acid (2S,3R)-3-(4-methoxy-benzyloxy)-2,3,7-trimethyl-1-(1-methylene-heptyl)-oct-6-enyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / diethyl ether

2: 93 percent / CSA / CH₂Cl₂

3: 86 percent / DIBAL / CH₂Cl₂

4: NMO, TPAP

5: 1.) t-BuLi

6: 70 percent / Et₃N, DMAP / CH₂Cl₂

With dmap; N-methyl-2-indolinone; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; tert.-butyl lithium; diisobutylaluminium hydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(99)00207-5