2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

Base Information

Chemical Name:2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid
CAS No.:1354438-99-5
Molecular Formula:C₁₂H₁₁Cl₃N₂O₄S
Molecular Weight:385.655
Hs Code.:

Synonyms:2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

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Chemical Property of 2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

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Technology Process of 2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

There total 1 articles about 2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354438-71-3
ethyl 2-((N-(2,4,6-trichlorophenyl)sulfamoyl)amino)acetate

: 1354438-99-5
2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / -20 - 20 °C / Inert atmosphere

2: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 5 h / 20 °C

With lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol;

Reference yield: 39.0%

: 4-aminotricyclo[3.3.1.13.7]decane-1-carboxamide hydrochloride

: 1354438-99-5
2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

: (trans)-4-(2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetamido)adamantan-1-carboxamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 12h;

Reference yield:

: 1354438-99-5
2-(4-methylene-1,1-dioxido-6-(2,4,6-trichlorophenyl)-1,2,6-thiadiazinan-2-yl)acetic acid

: 4-aminotricyclo[3,3,1,1(3,7)]decane-1-carboxamide hydrochloride

: C₂₃H₂₇Cl₃N₄O₄S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; isopropyl alcohol; at 20 ℃; for 5h;
DOI:10.1021/ml200226x