1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

Base Information

Chemical Name:1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose
CAS No.:405290-27-9
Molecular Formula:C₂₃H₃₁NO₁₁
Molecular Weight:497.499
Hs Code.:

Synonyms:1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

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Chemical Property of 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

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Technology Process of 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

There total 4 articles about 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 405290-25-7
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylideneamino)-β-D-glucopyranose

: 405290-27-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1081/CAR-100108272

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 405290-27-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaOH / H₂O / 18 h / 20 °C

2: pyridine / 18 h / 20 °C

3: 5.91 g / NaBH₃CN / tetrahydrofuran; H₂O / 1 h / 20 °C

With pyridine; sodium hydroxide; sodium cyanoborohydride; In tetrahydrofuran; water;
DOI:10.1081/CAR-100108272

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 405290-27-9
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,4-dimethoxybenzylamino)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaOH / H₂O / 18 h / 20 °C

2: pyridine / 18 h / 20 °C

3: 5.91 g / NaBH₃CN / tetrahydrofuran; H₂O / 1 h / 20 °C

With pyridine; sodium hydroxide; sodium cyanoborohydride; In tetrahydrofuran; water;
DOI:10.1081/CAR-100108272