(Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl

Base Information

• Chemical Name: (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl
• CAS No.: 1452822-23-9
• Molecular Formula: C₃₁H₃₅F₃O₂
• Molecular Weight: 496.613

Synonyms:(Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl

Chemical Property of (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl

Chemical Property:

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Technology Process of (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl

There total 7 articles about (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-(1-methylpropyl)phenol (99-71-8) + C21H23BrF4O (1452822-15-9) → (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl (1452822-23-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 80 ℃; stereoselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201203315

Reference yield:

1-bromo-4-(3-bromo-2,2,3,3-tetrafluoropropyl)benzene (842141-92-8) → (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl (1452822-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 80 °C / Schlenk technique; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide; 1: |Suzuki Coupling;

DOI:10.1002/chem.201203315

Reference yield:

4-hexyloxyphenylboronic acid (121219-08-7) → (Z)-4-(3-(4-sec-butylphenoxy)-2,3,3-trifluoroprop-1-enyl)-4'-(hexyloxy)biphenyl (1452822-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 80 °C / Schlenk technique; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide; 1: |Suzuki Coupling;

DOI:10.1002/chem.201203315

upstream raw materials:

1-bromo-4-(3-bromo-2,2,3,3-tetrafluoropropyl)benzene

4-(1-methylpropyl)phenol

C₂₁H₂₃BrF₄O

4-hexyloxyphenylboronic acid

Downstream raw materials:

4-(3-(4-sec-butylphenoxy)-3,3-difluoroprop-1-ynyl)-4'-(hexyloxy)biphenyl

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