1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol

Base Information

• Chemical Name: 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol
• CAS No.: 528559-67-3
• Molecular Formula: C₂₂H₄₁NO₃Si
• Molecular Weight: 395.658

Synonyms:1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol

Chemical Property of 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol

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Technology Process of 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol

There total 1 articles about 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.9%

2,4-dideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)-methyl]-2,4-dimethyl-L-arabinose (212703-47-4) → 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol (528559-67-3)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; methylamine; In tetrahydrofuran;

Reference yield: 94.5%

1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-1-(methylamino)-L-arabinitol (528559-67-3) + (2R,3S,4R,5S,6S,7Z)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[(4-methoxyphenyl)methoxy]-2,4,6-trimethyl-7,9-decadienoic acid (528559-72-0) + benzotriazol-1-yl-oxyl-tris(dimethyamino)phosphonium hexafluorophosphate (BOP) → 1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-1-[[(2R,3S,4R,5S,6S,7Z)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[(4-methoxyphenyl)methoxy]-2,4,6-trimethyl-1-oxo-7,9-decadienyl]methylamino]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-L-arabinitol (528559-73-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

upstream raw materials:

2,4-dideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-5-O-[(4-methoxyphenyl)-methyl]-2,4-dimethyl-L-arabinose

Downstream raw materials:

1,2,4-trideoxy-3-O-[(1,1-dimethylethyl)dimethylsilyl]-1-[[(2R,3S,4R,5S,6S,7Z)-3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-5-[(4-methoxyphenyl)methoxy]-2,4,6-trimethyl-1-oxo-7,9-decadienyl]methylamino]-5-O-[(4-methoxyphenyl)methyl]-2,4-dimethyl-L-arabinitol

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