C₂₃H₂₇NO₄Se

Base Information

Chemical Name:C₂₃H₂₇NO₄Se
CAS No.:1027068-83-2
Molecular Formula:C₂₃H₂₇NO₄Se
Molecular Weight:460.432
Hs Code.:

C<sub>23</sub>H<sub>27</sub>NO<sub>4</sub>Se

Synonyms:C₂₃H₂₇NO₄Se

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Chemical Property of C₂₃H₂₇NO₄Se

Chemical Property:

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Technology Process of C₂₃H₂₇NO₄Se

There total 5 articles about C₂₃H₂₇NO₄Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5414-21-1
5-bromopentan-1-nitrile

: 1027068-83-2
C₂₃H₂₇NO₄Se

Guidance literature:: Multi-step reaction with 6 steps

1: DIBAL-H / CH₂Cl₂ / 1 h / -68 °C

2: tetrahydrofuran / 0.33 h / -78 °C

3: 99 percent / tetramethylguanidinium azide / CH₂Cl₂ / 70 h / Ambient temperature

4: 1.) SnCl₂, 2.) aq. NaHCO₃ / 1.) MeOH, H₂O, r.t., overnight, 2.) dioxane, r.t., 5 h

5: 54 percent / PPTS / toluene / 1.25 h / Heating

6: NaHCO₃, NaIO₄ / methanol; H₂O / 1 h / Ambient temperature

With sodium periodate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium hydrogencarbonate; tetramethylguanidinum azide; tin(ll) chloride; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/p19960000123

Reference yield:

: 1191-30-6
5-bromopentanal

: 1027068-83-2
C₂₃H₂₇NO₄Se

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 0.33 h / -78 °C

2: 99 percent / tetramethylguanidinium azide / CH₂Cl₂ / 70 h / Ambient temperature

3: 1.) SnCl₂, 2.) aq. NaHCO₃ / 1.) MeOH, H₂O, r.t., overnight, 2.) dioxane, r.t., 5 h

4: 54 percent / PPTS / toluene / 1.25 h / Heating

5: NaHCO₃, NaIO₄ / methanol; H₂O / 1 h / Ambient temperature

With sodium periodate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; tetramethylguanidinum azide; tin(ll) chloride; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/p19960000123

Reference yield:

: 174744-02-6
7-Bromohept-1-en-3-ol

: 1027068-83-2
C₂₃H₂₇NO₄Se

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / tetramethylguanidinium azide / CH₂Cl₂ / 70 h / Ambient temperature

2: 1.) SnCl₂, 2.) aq. NaHCO₃ / 1.) MeOH, H₂O, r.t., overnight, 2.) dioxane, r.t., 5 h

3: 54 percent / PPTS / toluene / 1.25 h / Heating

4: NaHCO₃, NaIO₄ / methanol; H₂O / 1 h / Ambient temperature

With sodium periodate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; tetramethylguanidinum azide; tin(ll) chloride; In methanol; dichloromethane; water; toluene;
DOI:10.1039/p19960000123