(2S,3R)-3-phenyloxirane-2-carboxamide

Base Information

Chemical Name:(2S,3R)-3-phenyloxirane-2-carboxamide
CAS No.:1184725-14-1
Molecular Formula:C₉H₉NO₂
Molecular Weight:163.176
Hs Code.:

Synonyms:(2S,3R)-3-phenyloxirane-2-carboxamide

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Chemical Property of (2S,3R)-3-phenyloxirane-2-carboxamide

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Technology Process of (2S,3R)-3-phenyloxirane-2-carboxamide

There total 3 articles about (2S,3R)-3-phenyloxirane-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 621-79-4,22031-64-7
cinnamamide

: 1184725-14-1
(2S,3R)-3-phenyloxirane-2-carboxamide

Guidance literature:: With 2-Ethylhexanoic acid; dihydrogen peroxide; C₂₆H₃₆F₆MnN₆O₆S₂; In acetonitrile; at -40 ℃; for 2h; Reagent/catalyst; enantioselective reaction;
DOI:10.1002/adsc.202100198

Reference yield:

: 1201890-32-5
2,2,2-trichloro-1-((2R,3S)-3-phenyloxiran-2-yl)ethanone

: 1184725-14-1
(2S,3R)-3-phenyloxirane-2-carboxamide

: 189161-37-3
(2R,3S)-3-phenyloxirane-2-carboxamide

Guidance literature:: With ammonia; water; In acetonitrile; at 20 ℃; for 1h; optical yield given as %ee;
DOI:10.1002/adsc.200900041

Reference yield:

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 1184725-14-1
(2S,3R)-3-phenyloxirane-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / tert-butyl methyl ether / 0 - 20 °C

2: dihydrogen peroxide; 2-Ethylhexanoic acid; C₂₆H₃₆F₆MnN₆O₆S₂ / acetonitrile / 2 h / -40 °C

With ammonium hydroxide; 2-Ethylhexanoic acid; dihydrogen peroxide; C₂₆H₃₆F₆MnN₆O₆S₂; In tert-butyl methyl ether; acetonitrile;
DOI:10.1002/adsc.202100198