N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

Base Information

Chemical Name:N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)
CAS No.:246872-23-1
Molecular Formula:C₂₅H₁₅F₁₂N
Molecular Weight:557.382
Hs Code.:

Synonyms:N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

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Chemical Property of N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

Chemical Property:

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Technology Process of N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

There total 3 articles about N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 21450-64-6
(2,6-dimethylphenyl)magnesium bromide

: 246872-13-9
3,3',5,5'-tetrakis(trifluoromethyl)benzophenone O-p-tolylsulfonyloxime

: 246872-23-1
N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

Guidance literature:: In diethyl ether; toluene; at 25 ℃; for 0.5h;
DOI:10.1246/bcsj.72.1869

Reference yield:

: 175136-66-0
3,3',5,5'-tetrakis(trifluoromethyl)benzophenone(bis[3,5-bis(trifluoromethyl)phenyl])methanone

: 246872-23-1
N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / hydroxylammonium chloride; pyridine / 0.5 h / Heating

2: 97 percent / triethylamine / CH₂Cl₂ / 3 h / 25 °C

3: 90 percent / toluene; diethyl ether / 0.5 h / 25 °C

With pyridine; hydroxylamine hydrochloride; triethylamine; In diethyl ether; dichloromethane; toluene; 1: Condensation / 2: Tosylation / 3: Substitution;
DOI:10.1246/bcsj.72.1869

Reference yield:

: 246872-11-7
3,3',5,5'-tetrakis(trifluoromethyl)benzophenone oxime

: 246872-23-1
N-{bis[3,5-bis(trifluoromethyl)phenyl]methylidene}(2,6-dimethylaniline)

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / triethylamine / CH₂Cl₂ / 3 h / 25 °C

2: 90 percent / toluene; diethyl ether / 0.5 h / 25 °C

With triethylamine; In diethyl ether; dichloromethane; toluene; 1: Tosylation / 2: Substitution;
DOI:10.1246/bcsj.72.1869