methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

Base Information

Chemical Name:methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)
CAS No.:1320281-34-2
Molecular Formula:C₃₀H₃₂O₇S
Molecular Weight:536.646
Hs Code.:

Synonyms:methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

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Technology Process of methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

There total 8 articles about methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: p-methylphenyl 4,6-O-benzylidene-1-thio-β-D-mannopyranoside

: 1320281-34-2
methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol / 20 °C

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 20 °C

5: pyridine / 0 - 20 °C

With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol2016862

Reference yield:

: C₂₇H₂₈O₆S

: 1320281-34-2
methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: pyridine / 0 - 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ol2016862

Reference yield:

: 1320281-40-0
p-tolyl 2,3-di-O-benzyl-1-thio-α-D-mannopyranoside

: 1320281-34-2
methyl (p-tolyl 4-O-acetyl-2,3-di-O-benzyl-1-thio-α-D-mannopyranosyl uronate)

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: pyridine / 0 - 20 °C

With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol2016862