C₁₆H₁₄Cl₂FNO₄

Base Information

Chemical Name:C₁₆H₁₄Cl₂FNO₄
CAS No.:1429297-50-6
Molecular Formula:C₁₆H₁₄Cl₂FNO₄
Molecular Weight:374.196
Hs Code.:

C<sub>16</sub>H<sub>14</sub>Cl<sub>2</sub>FNO<sub>4</sub>

Synonyms:C₁₆H₁₄Cl₂FNO₄

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Chemical Property of C₁₆H₁₄Cl₂FNO₄

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Technology Process of C₁₆H₁₄Cl₂FNO₄

There total 4 articles about C₁₆H₁₄Cl₂FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 877397-65-4
(S)‐1‐(2,6-dichloro-3-fluorophenyl)ethanol

: 142063-12-5
methyl 5-hydroxy-2-methoxypyridinecarboxylate

: 1429297-50-6
C₁₆H₁₄Cl₂FNO₄

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2013.02.037

Reference yield:

: 54916-66-4
5-bromo-2-methoxy-nicotinic acid

: 1429297-50-6
C₁₆H₁₄Cl₂FNO₄

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; 1,10-Phenanthroline; caesium carbonate / toluene / 110 °C

2: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 55 °C

3: palladium on activated charcoal; hydrogen / methanol

4: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 0 - 20 °C

With copper(l) iodide; 1,10-Phenanthroline; oxalyl dichloride; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen; caesium carbonate; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.02.037

Reference yield:

: C₁₄H₁₃NO₄

: 1429297-50-6
C₁₆H₁₄Cl₂FNO₄

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 55 °C

2: palladium on activated charcoal; hydrogen / methanol

3: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 0 - 20 °C

With oxalyl dichloride; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.02.037