(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

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Chemical Name:(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate
CAS No.:1369377-66-1
Molecular Formula:C₃₂H₄₅BrN₄O₅
Molecular Weight:645.637
Hs Code.:

(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

Synonyms:(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

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Chemical Property of (S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

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Technology Process of (S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

There total 2 articles about (S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 6926-45-0
1-azidohexane

: 1365570-68-8
N-[3-bromo-5-(S)-menthoxy-2(5H)-furanonyl] (S)-phenylalanine propargyl ester

: 1369377-66-1
(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

Guidance literature:: With copper(II) acetate monohydrate; copper; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2012.01.092

Reference yield:

: 1283058-37-6
C₂₃H₃₀BrNO₅

: 1369377-66-1
(S)-(1-hexyl-1H-1,2,3-triazol-4-yl)methyl 2-((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-ylamino)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.5 h / Inert atmosphere

1.2: 8 h / 40 °C / Inert atmosphere

2.1: copper(II) acetate monohydrate; copper / acetonitrile / 4 h / 20 °C

With copper(II) acetate monohydrate; copper; potassium carbonate; In acetonitrile;
DOI:10.1016/j.tet.2012.01.092