p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside
CAS No.:1185868-63-6
Molecular Formula:C₅₃H₅₀N₂O₁₆
Molecular Weight:970.984
Hs Code.:

p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

Synonyms:p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

There total 4 articles about p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1185868-60-3
p-methoxyphenyl (4,6-O-benzylidene-2-deoxy-3-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

: 1185868-63-6
p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 4 ℃; for 2h;
DOI:10.1002/chem.201303474

Reference yield: 64.0%

: 617-86-7
triethylsilane

: 1185868-60-3
p-methoxyphenyl (4,6-O-benzylidene-2-deoxy-3-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

: 1185868-63-6
p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

: C₅₉H₆₄N₂O₁₆Si

Guidance literature:: With hafnium tetrakis(trifluoromethanesulfonate); In acetonitrile; at 4 ℃; for 0.5h; regioselective reaction;
DOI:10.1016/j.tetlet.2013.10.011

Reference yield:

: 1228362-90-0
3-O-acetyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranosyl trichloroacetimidate

: 1185868-63-6
p-methoxyphenyl (6-O-benzyl-2-deoxy-3-O-acetyl-2-phthalimido-α-D-glucopyranosyl)-(1→4)-2-deoxy-3-O-acetyl-6-O-benzyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 12 h / -60 °C

2: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 4 °C

With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1002/chem.201303474