N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

Base Information

Chemical Name:N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine
CAS No.:1608462-51-6
Molecular Formula:C₄₂H₃₈BNO₂
Molecular Weight:599.58
Hs Code.:

Synonyms:N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

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Chemical Property of N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

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Technology Process of N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

There total 5 articles about N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 4,4,5,5-tetramethyl-2-(4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)-1,3,2-dioxaborolane

: 1608462-50-5
4-([1,1'-biphenyl]-4-yl([1,1':3',1-terphenyl]-2'-yl)amino)phenyl trifluoromethanesulfonate

: 1608462-51-6
N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; water; for 12h; Inert atmosphere; Reflux;

Reference yield:

: 1608462-49-2
N-([1,1'-biphenyl]-4-yl)-N-(4-methoxyphenyl)-[1,1':3',1-terphenyl]-2'-amine

: 1608462-51-6
N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine hydrochloride / dichloromethane / Inert atmosphere; Reflux

1.2: 14 h / 0 - 20 °C

2.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 12 h / Inert atmosphere; Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; pyridine hydrochloride; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 1608462-47-0
N-([1,1'-biphenyl]-4-yl)-[1,1':3',1-terphenyl]-2'-amine

: 1608462-51-6
N-([1,1'-biphenyl]-4-yl)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-[1,1':3',1-terphenyl]-2'-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 72.5 h / Inert atmosphere; Reflux

2.1: pyridine hydrochloride / dichloromethane / Inert atmosphere; Reflux

2.2: 14 h / 0 - 20 °C

3.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 12 h / Inert atmosphere; Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 18-crown-6 ether; potassium acetate; pyridine hydrochloride; copper; potassium carbonate; In 1,4-dioxane; dichloromethane; water; 1,2-dichloro-benzene;