3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

Base Information

Chemical Name:3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester
CAS No.:113727-06-3
Molecular Formula:C₂₉H₃₃NO₁₂
Molecular Weight:587.581
Hs Code.:

Synonyms:3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

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Chemical Property of 3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

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Technology Process of 3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

There total 3 articles about 3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 21209-51-8
N-(Benzyloxycarbonyl)-L-serin-benzylester

: 4049-33-6
tetra-O-acetyl-β-D-xylopyranose

: 113727-06-3
3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 2h; Ambient temperature;

Reference yield: 44.0%

: 2771-53-1
ethyl 2,3,4-tri-O-acetyl-1-thio-β-D-xylopyranoside

: 21209-51-8
N-(Benzyloxycarbonyl)-L-serin-benzylester

: 113727-06-3
3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

Guidance literature:: With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In acetonitrile; for 1h; Ambient temperature;

Reference yield:

: 4049-33-6
tetra-O-acetyl-β-D-xylopyranose

: 113727-06-3
3-O-(2,3,4-Tri-O-acetyl-β-D-xylopyranosyl)-N-(benzyloxycarbonyl)-L-serin-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₄ / 1,2-dichloro-ethane / 0.75 h / -30 - -15 °C

2: 44 percent / DMTST / acetonitrile / 1 h / Ambient temperature

With tin(IV) chloride; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In 1,2-dichloro-ethane; acetonitrile;