C₂₅H₃₃NO₃S₃

Base Information

Chemical Name:C₂₅H₃₃NO₃S₃
CAS No.:1311280-85-9
Molecular Formula:C₂₅H₃₃NO₃S₃
Molecular Weight:491.74
Hs Code.:

C<sub>25</sub>H<sub>33</sub>NO<sub>3</sub>S<sub>3</sub>

Synonyms:C₂₅H₃₃NO₃S₃

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Chemical Property of C₂₅H₃₃NO₃S₃

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Technology Process of C₂₅H₃₃NO₃S₃

There total 7 articles about C₂₅H₃₃NO₃S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1311280-83-7
C₂₅H₃₁NO₃S₃

: 1311280-84-8
C₂₅H₃₃NO₃S₃

: 1311280-85-9
C₂₅H₃₃NO₃S₃

Guidance literature:: With borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol2010598

Reference yield:

: 1311280-65-5
C₃₄H₅₃NO₃S₅Si

: 1311280-85-9
C₂₅H₃₃NO₃S₃

Guidance literature:: Multi-step reaction with 5 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

4: 2,6-dimethylpyridine; mercury(II) perchlorate / tetrahydrofuran; water / 0.5 h / 0 °C / Inert atmosphere

5: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; mercury(II) perchlorate; borane-THF; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; water;
DOI:10.1021/ol2010598

Reference yield:

: 1311280-53-1
C₂₈H₃₉NO₃S₅

: 1311280-85-9
C₂₅H₃₃NO₃S₃

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

3: 2,6-dimethylpyridine; mercury(II) perchlorate / tetrahydrofuran; water / 0.5 h / 0 °C / Inert atmosphere

4: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; mercury(II) perchlorate; borane-THF; sodium hydride; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; water;
DOI:10.1021/ol2010598