(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

Base Information

Chemical Name:(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide
CAS No.:1093131-23-7
Molecular Formula:C₂₇H₃₈N₂O₅
Molecular Weight:470.609
Hs Code.:

Synonyms:(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

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Chemical Property of (R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

Chemical Property:

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Technology Process of (R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

There total 5 articles about (R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093131-52-2
(R)-3-methoxy-2-methylbenzoic acid N-(1-tert-butylbutyl)hydrazide

: 34523-76-7
3,5-dimethoxy-4-methylbenzoyl chloride

: 1093131-23-7
(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

Guidance literature:: With potassium carbonate; In dichloromethane; water; at 20 ℃;

Reference yield:

: 740799-69-3
3-methoxy-2-methyl-benzoic acid hydrazide

: 1093131-23-7
(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / methanol / 8 h / Heating / reflux

2: dichloromethane / 4 h / 5 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2.5 h / 2844.39 Torr

4: potassium carbonate / dichloromethane; water / 20 °C

With hydrogen; potassium carbonate; acetic acid; palladium 10% on activated carbon; In methanol; dichloromethane; water;

Reference yield:

: 1093131-50-0
3-methoxy-2-methylbenzoic acid (2,2-dimethylpropylidene)hydrazide

: 1093131-23-7
(R)-3,5-dimethoxyl-4-methylbenzoic acid N-(1-tert-butylbutyl)-N'-(3-methoxy-2-methylbenzoyl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 4 h / 5 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 2.5 h / 2844.39 Torr

3: potassium carbonate / dichloromethane; water / 20 °C

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol; dichloromethane; water;