C₂₉H₃₀O₉S

Base Information Edit

Chemical Name:C₂₉H₃₀O₉S
CAS No.:73957-98-9
Molecular Formula:C₂₉H₃₀O₉S
Molecular Weight:554.618
Hs Code.:
Mol file:73957-98-9.mol

C<sub>29</sub>H<sub>30</sub>O<sub>9</sub>S

Synonyms:C₂₉H₃₀O₉S

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Chemical Property of C₂₉H₃₀O₉S Edit

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Technology Process of C₂₉H₃₀O₉S

There total 6 articles about C₂₉H₃₀O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 73957-97-8
C₂₂H₂₄O₇

: 98-59-9
p-toluenesulfonyl chloride

: 73957-98-9
C₂₉H₃₀O₉S

Guidance literature:: With pyridine; 1.) 23 deg C, 6 h, 2.) 50 deg C, 3h;
DOI:10.1021/ja00524a045

Reference yield:

: 55797-81-4,105453-39-2
C₂₆H₂₂O₈

: 73957-98-9
C₂₉H₃₀O₉S

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / benzoic acid / 1,2-dimethoxy-ethane / 4 h / Heating

2: 100 percent / H₂SO₄ / 3 h / 23 °C

3: 93 percent / 95percent zinc amalgam, dry hydrogen chloride / diethyl ether / 6 h / 15 °C

4: 100 percent / H₂ / 10percent Pd/C / methanol / 23 °C

5: 99 percent / dry hydroden chloride / 72 h / 23 °C

6: 98 percent / pyridine / 1.) 23 deg C, 6 h, 2.) 50 deg C, 3h

With pyridine; hydrogenchloride; amalgamated zinc; sulfuric acid; hydrogen; benzoic acid; palladium on activated charcoal; In methanol; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/ja00524a045

Reference yield:

: 73957-95-6,74006-65-8
C₃₂H₃₀O₁₀

: 73957-98-9
C₂₉H₃₀O₉S

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / 95percent zinc amalgam, dry hydrogen chloride / diethyl ether / 6 h / 15 °C

2: 100 percent / H₂ / 10percent Pd/C / methanol / 23 °C

3: 99 percent / dry hydroden chloride / 72 h / 23 °C

4: 98 percent / pyridine / 1.) 23 deg C, 6 h, 2.) 50 deg C, 3h

With pyridine; hydrogenchloride; amalgamated zinc; hydrogen; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/ja00524a045