p-Methoxy phenyl allenyl ether

Base Information

Chemical Name:p-Methoxy phenyl allenyl ether
CAS No.:66397-26-0
Molecular Formula:C₁₀H₁₀O₂
Molecular Weight:162.188
Hs Code.:

Synonyms:p-Methoxy phenyl allenyl ether

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Chemical Property of p-Methoxy phenyl allenyl ether

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Technology Process of p-Methoxy phenyl allenyl ether

There total 2 articles about p-Methoxy phenyl allenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 17061-86-8
1-methoxy-4-(2-propynyloxy)benzene

: 66397-26-0
p-Methoxy phenyl allenyl ether

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; for 0.0333333h; microwave irradiation;
DOI:10.1080/00397919708005453

Reference yield:

: 150-76-5
4-methoxy-phenol

: 66397-26-0
p-Methoxy phenyl allenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / Reflux

2: potassium tert-butylate / dimethyl sulfoxide / 1.5 h / 20 °C

With potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; acetone;
DOI:10.1007/s00706-010-0406-1

Reference yield: 97.0%

: 66397-26-0
p-Methoxy phenyl allenyl ether

: 4559-70-0
Diphenylphosphine oxide

: (R)-(1-(4-methoxyphenoxy)allyl)diphenylphosphine oxide

Guidance literature:: With (R)-(-)-5,5’-bis(diphenyl;phosphine)-2,2,2’,2’-tetrafluoro-4,4’-bi-1,3-benzodioxole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1002/anie.202112285