Technology Process of 1,3-Benzodioxol-4-amine,N-butyl-6-ethyl-(9CI)
There total 6 articles about 1,3-Benzodioxol-4-amine,N-butyl-6-ethyl-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 93 percent / aq. HBr; AcOH / 7 h / Heating
2: 28 percent / Adogen 464; aq. NaOH / 6 h / Heating
3: 100 percent / H2 / Pd/C / ethanol / 6 h / 2585.74 - 2844.31 Torr
4: Na2SO4 / methanol / 1 h / Heating
5: 129 mg / NaBH4 / methanol
With
sodium hydroxide; sodium tetrahydroborate; adogen 464; hydrogen bromide; hydrogen; acetic acid; sodium sulfate;
palladium on activated charcoal;
In
methanol; ethanol;
DOI:10.1021/ja0214274
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / H2 / Pd/C / ethanol / 6 h / 2585.74 - 2844.31 Torr
2: Na2SO4 / methanol / 1 h / Heating
3: 129 mg / NaBH4 / methanol
With
sodium tetrahydroborate; hydrogen; sodium sulfate;
palladium on activated charcoal;
In
methanol; ethanol;
DOI:10.1021/ja0214274
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 28 percent / Adogen 464; aq. NaOH / 6 h / Heating
2: 100 percent / H2 / Pd/C / ethanol / 6 h / 2585.74 - 2844.31 Torr
3: Na2SO4 / methanol / 1 h / Heating
4: 129 mg / NaBH4 / methanol
With
sodium hydroxide; sodium tetrahydroborate; adogen 464; hydrogen; sodium sulfate;
palladium on activated charcoal;
In
methanol; ethanol;
DOI:10.1021/ja0214274
