Technology Process of (R,R,R,R)-N(1)-benzyl-2-(acetoxymethyl)-3-benzyloxy-4,5-diacetoxypiperidine
There total 1 articles about (R,R,R,R)-N(1)-benzyl-2-(acetoxymethyl)-3-benzyloxy-4,5-diacetoxypiperidine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(1S,2R,3R,4R,5S)-N(1)-benzyl-2-[(triisopropylsilyloxy)methyl]-3-benzyloxy-4-hydroxy-1-azabicyclo[3.1.0]hexanium tetrafluoroborate;
With
water;
In
1,4-dioxane;
at 20 ℃;
for 16h;
With
pyridine; pyridine hydrogenfluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 16h;
acetic anhydride;
With
pyridine; dmap;
at 0 - 20 ℃;
for 16h;
DOI:10.1016/j.tet.2014.03.100
![(1S,2R,3R,4R,5S)-N<sup>(1)</sup>-benzyl-2-[(triisopropylsilyloxy)methyl]-3-benzyloxy-4-hydroxy-1-azabicyclo[3.1.0]hexanium tetrafluoroborate](/Databaselist/images/loading.webp)
