Technology Process of N-(Bicyclo<3.1.0>hex-exo-6-yl)-3,5-dinitro-N-nitrosobenzamid
There total 5 articles about N-(Bicyclo<3.1.0>hex-exo-6-yl)-3,5-dinitro-N-nitrosobenzamid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; sodium nitrite;
In
acetic anhydride;
at 0 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 82 percent / pyridine / 1.) 30 min, room temp.; 2.) 45 min, 40 deg C
2: 94 percent / glacial acetic acid, NaNO2 / acetic anhydride / 4 h / 0 °C
With
pyridine; acetic acid; sodium nitrite;
In
acetic anhydride;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / H2O; acetone / 0.5 h / 0 °C
2: sodium azide / acetone; H2O / 1 h / 0 °C
3: 2.) conc. HCl / 1.) toluene, 30 min, heating; 2.) toluene, 15 min, room temp.
4: 82 percent / pyridine / 1.) 30 min, room temp.; 2.) 45 min, 40 deg C
5: 94 percent / glacial acetic acid, NaNO2 / acetic anhydride / 4 h / 0 °C
With
pyridine; hydrogenchloride; sodium azide; acetic acid; triethylamine; sodium nitrite;
In
water; acetic anhydride; acetone;
