3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride

Base Information

• Chemical Name: 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride
• CAS No.: 130245-59-9
• Molecular Formula: C₃₁H₂₇N₇O₆*ClH
• Molecular Weight: 630.06
• Mol file: 130245-59-9.mol

Synonyms:3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride

Chemical Property of 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride

There total 7 articles about 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-<3-nitrobenzamido>benzoic acid (106590-58-3) → 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride (130245-59-9)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂

2: Et₃N / tetrahydrofuran / 12 h / Ambient temperature

3: 1.) HCl(gas), 2.) NH₃(gas) / 1.) ethanol, RT, 3 h, 2.) RT, 2 h

With hydrogenchloride; thionyl chloride; ammonia; triethylamine; In tetrahydrofuran;

Reference yield:

3-<3-nitrobenzamido>benzoyl chloride (16360-90-0) → 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride (130245-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 12 h / Ambient temperature

2: 1.) HCl(gas), 2.) NH₃(gas) / 1.) ethanol, RT, 3 h, 2.) RT, 2 h

With hydrogenchloride; ammonia; triethylamine; In tetrahydrofuran;

Reference yield:

meta-aminobenzoic acid (99-05-8,159139-79-4) → 3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride (130245-59-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 88 percent / 4percent aq. NaHCO₃ / acetone / 12 h / Ambient temperature

2: SOCl₂

3: Et₃N / tetrahydrofuran / 12 h / Ambient temperature

4: 1.) HCl(gas), 2.) NH₃(gas) / 1.) ethanol, RT, 3 h, 2.) RT, 2 h

With hydrogenchloride; thionyl chloride; ammonia; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; acetone;

upstream raw materials:

3-<3-<3-(3-nitrobenzamido)benzamido>benzamido>benzamidopropionitrile

3-<3-nitrobenzamido>benzoic acid

3-<3-nitrobenzamido>benzoyl chloride

3-<3-(3-nitrobenzene-1-carboxamido)benzene-1-carboxamido>propionitrile

Downstream raw materials:

3-<3-<3-(3-aminobenzamido)benzamido>benzamido>benzamidopropionamidine hydrochloride