2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

Base Information

Chemical Name:2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide
CAS No.:1011722-60-3
Molecular Formula:C₁₆H₁₉NSe
Molecular Weight:304.294
Hs Code.:

Synonyms:2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

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Chemical Property of 2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

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Technology Process of 2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

There total 1 articles about 2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1666-13-3
diphenyl diselenide

: 2410-47-1
2-{2'-(N,N-dimethylamino)ethyl}bromobenzene

: 1011722-60-3
2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

Guidance literature:: 2-{2'-(N,N-dimethylamino)ethyl}bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -50 ℃; for 0.5h;

diphenyl diselenide; In tetrahydrofuran; hexane; at -30 - 20 ℃; for 17h; Further stages.;
DOI:10.1002/hc.20299

Reference yield: 50.0%

: 1011722-60-3
2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

: 1011722-54-5
2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenoxide

Guidance literature:: 2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide; With tert-butylhypochlorite; In methanol; at -50 ℃; for 0.666667h;

With sodium hydroxide; In methanol; Further stages.;
DOI:10.1002/hc.20299

Reference yield:

: 1011722-60-3
2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenide

: 1011722-70-5
(S)-(-)-2-{2'-(N,N-dimethylamino)ethyl}diphenyl selenoxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-butyl hypochlorite / methanol / 0.67 h / -50 °C

1.2: 50 percent / aq. NaOH / methanol

2.1: amylose carbamate derivative/silica gel(Daicel Chiralpak AS) / hexane; ethanol

With tert-butylhypochlorite; In methanol; ethanol; hexane;
DOI:10.1002/hc.20299