(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

Base Information

Chemical Name:(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid
CAS No.:1337570-42-9
Molecular Formula:C₁₈H₂₃N₃O₄
Molecular Weight:345.398
Hs Code.:

Synonyms:(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

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Chemical Property of (S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

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Technology Process of (S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

There total 4 articles about (S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1337570-28-1
(S)-benzyl 2-((2-((1-((benzyloxy)carbonyl)cyclopentyl)carbamoyl)phenyl)carbamoyl)pyrrolidine-1-carboxylate

: 1337570-42-9
(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; water; for 10h; Inert atmosphere;
DOI:10.1021/ol202284n

Reference yield:

: benzyl 1-amino-1-cyclopentanoate hydrochloride

: 1337570-42-9
(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethyl acetate / 10 h / Reflux; Inert atmosphere

2: pyridine; trichlorophosphate / -10 - -5 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethanol; water / 10 h / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; triethylamine; trichlorophosphate; In ethanol; water; ethyl acetate;
DOI:10.1021/ol202284n

Reference yield:

: 118-48-9
isatoic anhydride

: 1337570-42-9
(S)-1-(2-(pyrrolidine-2-carboxamido)benzamido)cyclopentanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethyl acetate / 10 h / Reflux; Inert atmosphere

2: pyridine; trichlorophosphate / -10 - -5 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethanol; water / 10 h / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; triethylamine; trichlorophosphate; In ethanol; water; ethyl acetate;
DOI:10.1021/ol202284n