Technology Process of tris(3-(bromomethyl)benzyl)amine
There total 3 articles about tris(3-(bromomethyl)benzyl)amine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
at 25 ℃;
Inert atmosphere;
DOI:10.1021/ja108212v
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-Bromosuccinimide; benzoic acid anhydride / tetrachloromethane / 6 h / Inert atmosphere; Reflux
2: ammonium hydroxide / 72 h / 20 °C / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C / Inert atmosphere
4: hydrogen bromide; acetic acid / 25 °C / Inert atmosphere
With
ammonium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; hydrogen bromide; acetic acid; benzoic acid anhydride;
In
tetrahydrofuran; tetrachloromethane;
DOI:10.1002/chem.201604598
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium hydroxide / 72 h / 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C / Inert atmosphere
3: hydrogen bromide; acetic acid / 25 °C / Inert atmosphere
With
ammonium hydroxide; lithium aluminium tetrahydride; hydrogen bromide; acetic acid;
In
tetrahydrofuran;
DOI:10.1002/chem.201604598
