(1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Base Information

• Chemical Name: (1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
• CAS No.: 196609-10-6
• Molecular Formula: C₂₄H₃₀O₃
• Molecular Weight: 366.5

Synonyms:(1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Chemical Property of (1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Chemical Property:

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Technology Process of (1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 1 articles about (1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (196609-10-6)

Guidance literature:

With pyridine N-oxide; In tetrahydrofuran; at 25 ℃; for 14h; Yield given;

DOI:10.1021/jo9708708

Reference yield:

(1S,2S)-2-Furan-2-yl-cyclopropanecarboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (196609-10-6) → Benzoic acid (1S,2S)-2-furan-2-yl-cyclopropylmethyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / LiAlH₄ / diethyl ether / 14 h / 35 °C

2: Et₃N, DMAP / 14 h / 25 °C

With dmap; lithium aluminium tetrahydride; triethylamine; In diethyl ether;

DOI:10.1021/jo9708708

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