1-Chloro-1,1,3,3-Tetraisopropyl Disiloxane

Base Information

• Chemical Name: 1-Chloro-1,1,3,3-Tetraisopropyl Disiloxane
• CAS No.: 116045-69-3
• Molecular Formula: C₁₂H₂₉ClOSi₂
• Molecular Weight: 280.986
• Mol file: 116045-69-3.mol

Synonyms:5-chlorotetraisopropyldisiloxane

Chemical Property of 1-Chloro-1,1,3,3-Tetraisopropyl Disiloxane

Chemical Property:

• Boiling Point: 90°C / 1

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Chloro-1,1,3,3-Tetraisopropyl Disiloxane

There total 1 articles about 1-Chloro-1,1,3,3-Tetraisopropyl Disiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

1,1,3,3-tetraisopropyldisiloxane (18043-71-5) → 5-chlorotetraisopropyldisiloxane (116045-69-3)

Guidance literature:

With trichloroisocyanuric acid; In tetrahydrofuran; at -80 - 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2018.08.022

Reference yield: 96.0%

rosuvastatin allyl ester (1352945-05-1) + 5-chlorotetraisopropyldisiloxane (116045-69-3) → C49H88FN3O8SSi4

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 16h;

Reference yield: 53.0%

acetic anhydride (108-24-7) + 5-chlorotetraisopropyldisiloxane (116045-69-3) + N-benzoyladenosine (4546-55-8) → C31H45N5O7Si2

Guidance literature:

5-chlorotetraisopropyldisiloxane; N-benzoyladenosine; With pyridine; at 20 ℃; for 3.5h; Cooling with ice;

acetic anhydride; at 20 ℃; for 13h;

upstream raw materials:

1,1,3,3-tetraisopropyldisiloxane

Refernces