(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

Base Information

Chemical Name:(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester
CAS No.:359406-65-8
Molecular Formula:C₂₃H₂₄O₃
Molecular Weight:348.442
Hs Code.:

Synonyms:(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

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Chemical Property of (E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

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Technology Process of (E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

There total 1 articles about (E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136314-66-4
methyl (3S,4E)-3-(dimethylphenylsilyl)-4-hexenoate

: C₂₃H₂₀O₂

: 359406-65-8
(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

Guidance literature:: C₂₃H₂₀O₂; With dicobalt octacarbonyl; at 20 ℃;

methyl (3S,4E)-3-(dimethylphenylsilyl)-4-hexenoate; With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃; for 12h;

With trimethylamine-N-oxide; In methanol; Further stages.;
DOI:10.1021/ol016016r

Reference yield:

: 359406-65-8
(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

: (2R,3R)-3-Benzyloxy-2-methyl-5-phenyl-pent-4-ynal

Guidance literature:: With dimethylsulfide; ozone; In methanol;
DOI:10.1021/ol016016r

Reference yield:

: 359406-65-8
(E)-(5S,6R)-6-Benzyloxy-5-methyl-8-phenyl-oct-3-en-7-ynoic acid methyl ester

: (2S,3R)-2-Methyl-5-phenyl-pent-4-yne-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: O₃; Me₂S / methanol

2: 80 percent / LiBH₄ / tetrahydrofuran

3: 50 percent / BCl₃; DCM

With lithium borohydride; dimethylsulfide; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; boron trichloride; ozone; In tetrahydrofuran; methanol;
DOI:10.1021/ol016016r