Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4]

Base Information

• Chemical Name: Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4]
• CAS No.: 566933-64-0
• Molecular Formula: C₁₅H₂₃BMnO₄P₂*C₃₂H₁₂BF₂₄
• Molecular Weight: 1258.26

Synonyms:Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4]

Chemical Property of Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4]

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Technology Process of Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4]

There total 2 articles about Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[Mn(CO)4(BH₃P(CH₃)3)(P(CH₃)2(C₆H₅))][B(C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Brookhart's acid + [Mn(CO)4(BH2P(CH3)3)(P(CH3)2C6H5)] → Mn(CO)4(BH3P(CH3)3)(P(CH3)2(C6H5))(1+)*B(C6H3(CF3)2)4(1-)=[Mn(CO)4(BH3P(CH3)3)(P(CH3)2(C6H5))][B(C6H3(CF3)2)4] (566933-64-0)

Guidance literature:

In dichloromethane-d2; mixed under vac., mixt. stirred for 3 h;

DOI:10.1002/anie.200219992

Reference yield:

Brookhart's acid + cis-[Mn(Me)(CO)4(PMe2Ph)] (20861-36-3,68852-71-1) + trimethylphosphine-borane (1898-77-7) → Mn(CO)4(BH3P(CH3)3)(P(CH3)2(C6H5))(1+)*B(C6H3(CF3)2)4(1-)=[Mn(CO)4(BH3P(CH3)3)(P(CH3)2(C6H5))][B(C6H3(CF3)2)4] (566933-64-0)

Guidance literature:

In diethyl ether; byproducts: CH4; BH3*P(CH3)3 added to Et2O soln. produced by reaction of Mn-complex with H(O(C2H5)2)2(B(C6H3(CF3)2)4;

DOI:10.1002/anie.200219992

upstream raw materials:

cis-[Mn(Me)(CO)4(PMe₂Ph)]

trimethylphosphine-borane

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