C₁₃H₁₈NO₁₃P₃

Base Information

Chemical Name:C₁₃H₁₈NO₁₃P₃
CAS No.:1428631-98-4
Molecular Formula:C₁₃H₁₈NO₁₃P₃
Molecular Weight:489.206
Hs Code.:

C<sub>13</sub>H<sub>18</sub>NO<sub>13</sub>P<sub>3</sub>

Synonyms:C₁₃H₁₈NO₁₃P₃

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Chemical Property of C₁₃H₁₈NO₁₃P₃

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Technology Process of C₁₃H₁₈NO₁₃P₃

There total 6 articles about C₁₃H₁₈NO₁₃P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1428631-94-0
C₁₃H₁₅NO₄

: 1428631-98-4
C₁₃H₁₈NO₁₃P₃

Guidance literature:: C₁₃H₁₅NO₄; With trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; at -15 - 10 ℃; Inert atmosphere;

With tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; In N,N-dimethyl-formamide; at -10 - 0 ℃; for 0.5h;
DOI:10.1021/ja312148q

Reference yield:

: 1364927-25-2
C₂₀H₂₃NO₆

: 1428631-98-4
C₁₃H₁₈NO₁₃P₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / 15 h / 20 °C / Inert atmosphere

2.1: triethylamine; palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

3.2: 0.67 h / 0 °C

3.3: 2.6 h / 0 - 20 °C

4.1: potassium fluoride; tetrabutylammomium bromide; palladium diacetate / water / 0.25 h / 150 °C / Microwave irradiation

5.1: sodium methylate / dichloromethane; methanol / 1 h / 5 - 20 °C

6.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

6.2: 0.5 h / -10 - 0 °C

With pyridine; trimethyl phosphite; hydrogenchloride; potassium fluoride; palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; sodium methylate; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; 3.2: |Sandmeyer Reaction / 3.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-84-8
C₂₈H₂₉NO₆

: 1428631-98-4
C₁₃H₁₈NO₁₃P₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

1.2: 0.67 h / 0 °C

1.3: 2.6 h / 0 - 20 °C

2.1: potassium fluoride; tetrabutylammomium bromide; palladium diacetate / water / 0.25 h / 150 °C / Microwave irradiation

3.1: sodium methylate / dichloromethane; methanol / 1 h / 5 - 20 °C

4.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

4.2: 0.5 h / -10 - 0 °C

With trimethyl phosphite; hydrogenchloride; potassium fluoride; tetrabutylammomium bromide; sodium methylate; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; 1.2: |Sandmeyer Reaction / 1.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q