ClPh₂SiGePh₃

Base Information

Chemical Name:ClPh₂SiGePh₃
CAS No.:149033-90-9
Molecular Formula:C₃₀H₂₅ClGeSi
Molecular Weight:521.657
Hs Code.:

Synonyms:ClPh₂SiGePh₃

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Chemical Property of ClPh₂SiGePh₃

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Technology Process of ClPh₂SiGePh₃

There total 2 articles about ClPh₂SiGePh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 57482-41-4
Triphenylgermyl-kalium

: 80-10-4
diphenylsilyl dichloride

: 149033-90-9
ClPh₂SiGePh₃

Guidance literature:: In diethyl ether; Ar; addition oh KGe(C6H5)3 to a solution of the silane at -78 ° C within 2 h; then stirring of the reaction mixture at room temperature for 3 h;; solvent removal; dilution of the residue in toluene; filtration; crystn. of (C6H5)3GeSi(C6H5)2Ge(C6H5)3; filtration; the filtrate is evaporated to dryness; dilution of the residue in ether; crystn. of the product; elem. anal.;;
DOI:10.1016/0022-328X(93)80184-D

Reference yield:

: 2816-39-9
hexaphenyldigermane

: 149033-90-9
ClPh₂SiGePh₃

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran

2: diethyl ether

In tetrahydrofuran; diethyl ether;
DOI:10.1016/0022-328X(93)80184-D

Reference yield: 41.0%

: 149033-90-9
ClPh₂SiGePh₃

: 15487-82-8,6735-25-7
triphenylsilylkalium

: 149033-87-4
Ph₃SiSiPh₂GePh₃

Guidance literature:: With HCl; In diethyl ether; -78 ° C; equimolar amounts; addition of KSiPh3 in ether to the germane in ether within 3 h; stirring was continued for 20 h at room temperature; solvent removal; dilution with hot benzene;; the solution is washed with water and dried over Na2SO4; filtration; solvent removal; recrystn of the product from toluene/heptane 2/1; elem. anal.;;
DOI:10.1016/0022-328X(93)80184-D