2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

Base Information

Chemical Name:2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone
CAS No.:155192-28-2
Molecular Formula:C₂₃H₃₆OSi₂
Molecular Weight:384.709
Hs Code.:

Synonyms:2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

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Chemical Property of 2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

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Technology Process of 2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

There total 8 articles about 2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 106-95-6
allyl bromide

: 155192-26-0
4-Trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

: 2-Allyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

: 155192-28-2
2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/0040-4039(94)85068-2

Reference yield:

: 1489-97-0
ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate

: 155192-28-2
2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

Guidance literature:: Multi-step reaction with 7 steps

1: LDA / tetrahydrofuran

2: diisobutylaluminium hydride / toluene

3: (COCl)2, DMSO, Et₃N / CH₂Cl₂

4: 97 percent / PPh₃ / CH₂Cl₂

5: 95 percent / n-butyl lithium / tetrahydrofuran

6: formic acid / petroleum ether

7: 15 percent / LDA / tetrahydrofuran

With n-butyllithium; formic acid; oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; Petroleum ether;
DOI:10.1016/0040-4039(94)85068-2

Reference yield:

: 17159-79-4
ethyl 4-oxocyclohexane-1-carboxylate

: 155192-28-2
2,2-Diallyl-4-trimethylsilanylethynyl-4-(3-trimethylsilanyl-prop-2-ynyl)-cyclohexanone

Guidance literature:: Multi-step reaction with 8 steps

1: CSA / toluene

2: LDA / tetrahydrofuran

3: diisobutylaluminium hydride / toluene

4: (COCl)2, DMSO, Et₃N / CH₂Cl₂

5: 97 percent / PPh₃ / CH₂Cl₂

6: 95 percent / n-butyl lithium / tetrahydrofuran

7: formic acid / petroleum ether

8: 15 percent / LDA / tetrahydrofuran

With n-butyllithium; formic acid; oxalyl dichloride; camphor-10-sulfonic acid; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; Petroleum ether;
DOI:10.1016/0040-4039(94)85068-2