N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Base Information

Chemical Name:N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide
CAS No.:1026618-53-0
Molecular Formula:C₂₃H₂₂N₄O₄
Molecular Weight:418.452
Hs Code.:

<i>N</i>-[4-(5-amino-1<i>H</i>-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Synonyms:N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

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Chemical Property of N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Chemical Property:

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Technology Process of N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

There total 5 articles about N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1025982-82-4
3,4,5-trimethoxy-N-[4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-benzamide

: 1026618-53-0
N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; at 80 ℃; for 16h;
DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 1026618-53-0
N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h / 20 °C

2: H₂ / Pd/C / methanol; tetrahydrofuran / 16 h / 80 °C

With pyridine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1026618-53-0
N-[4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-3,4,5-trimethoxy-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / polyphosphoric acid / xylene / 60 - 150 °C

2: pyridine / 3 h / 20 °C

3: H₂ / Pd/C / methanol; tetrahydrofuran / 16 h / 80 °C

With pyridine; PPA; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; xylene;
DOI:10.1016/j.ejmech.2006.03.014