methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

Base Information

Chemical Name:methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate
CAS No.:368448-91-3
Molecular Formula:C₂₇H₂₉NO₂
Molecular Weight:399.533
Hs Code.:

Synonyms:methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

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Technology Process of methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

There total 1 articles about methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 38447-05-1,38448-84-9,101934-35-4,121411-05-0,1516-24-1,24196-39-2
(2E,4E)-methyl 5-phenylpenta-2,4-dienoate

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 368448-91-3
methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

(2E,4E)-methyl 5-phenylpenta-2,4-dienoate; In tetrahydrofuran; at -78 ℃; for 2h; Further stages.;
DOI:10.1039/b100402f

Reference yield: 77.0%

: 368448-91-3
methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

: 170726-18-8
methyl (3S)-3-amino-5-phenylpentanoate

Guidance literature:: With ammonium formate; palladium dihydroxide; In methanol; for 0.75h; Heating;
DOI:10.1039/b100402f

Reference yield: 75.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 368448-91-3
methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate

: Benzyl-{(E)-(R)-1-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-3-phenyl-allyl}-((S)-1-phenyl-ethyl)-amine

Guidance literature:: methyl (3R,4E,αS)-3-(N-benzyl-N-α-methylbenzylamino)-5-phenylpent-4-enoate; With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃; for 2h;

tert-butylchlorodiphenylsilane; With 1H-imidazole; In tetrahydrofuran; at 20 ℃; for 6h; Further stages.;
DOI:10.1039/b100402f