(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Base Information

Chemical Name:(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide
CAS No.:1266347-59-4
Molecular Formula:C₂₄H₃₂N₂O₃S
Molecular Weight:428.596
Hs Code.:

Synonyms:(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Suppliers and Price of (S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

There total 5 articles about (S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₃NO₄S

: 103-67-3
benzyl-methyl-amine

: 1266347-59-4
(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol103105q

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 1266347-59-4
(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 60 °C

2.2: 6 h / 60 °C

3.1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 3 h / 0 - 20 °C

4.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; caesium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol103105q

Reference yield:

: 1266347-51-6
(S)-methyl 2-(N-(but-3-en-1-yl)phenylsulfonamido)-4-methylpentanoate

: 1266347-59-4
(S)-N-benzyl-2-(N-(but-3-en-1-yl)phenylsulfonamido)-N,4-dimethylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 3 h / 0 - 20 °C

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol103105q