Technology Process of C31H31N5O2
There total 13 articles about C31H31N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum(IV) oxide; 5%-palladium/activated carbon;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C
1.2: pH > 7 / Saturated solution
2.1: N,N-dimethyl-formamide / 20 - 80 °C
3.1: 6 h / 120 °C
4.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C
4.2: Saturated solution
5.1: acetic acid / ethanol / 5 h / 50 °C
6.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation
7.1: hydrogen / platinum(IV) oxide; 5%-palladium/activated carbon / methanol; dichloromethane
With
thionyl chloride; hydrazine monohydrobromide; hydrogen; potassium carbonate; acetic acid;
platinum(IV) oxide; tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 1.5 h / 20 °C
2: triethylamine / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 160 °C / Inert atmosphere; Microwave irradiation
3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation
4: hydrogen / platinum(IV) oxide; 5%-palladium/activated carbon / methanol; dichloromethane
With
hydrogen; potassium carbonate; triethylamine;
platinum(IV) oxide; tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
1,4-dioxane; methanol; dichloromethane; water;