CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁

Base Information

Chemical Name:CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁
CAS No.:65062-96-6
Molecular Formula:C₁₆H₂₂B₁₀O
Molecular Weight:338.46
Hs Code.:

CH<sub>3</sub>COC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>B<sub>10</sub>H<sub>11</sub>

Synonyms:CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁

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Chemical Property of CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁

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Technology Process of CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁

There total 1 articles about CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 23754-22-5
1-(4-bromophenyl)-m-carborane

: 149104-90-5
4-acetylphenylboronic acid

: 65062-96-6
CH₃COC₆H₄C₆H₄C₂B₁₀H₁₁

Guidance literature:: With K₂CO₃; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; water; toluene; (Ar); dissolving of BrC6H4C2B10H11 in THF/toluene, addn. of 4-acetylphenylboronic acid, PdCl2(PPh3)2 and aq. soln. of K2CO3, reflux at 100°C for 24 h; extn. with CH2Cl2, drying of combined org. layer over MgSO4, evapn. of solvent, chromy. on silica with 10-15% EtOAc in hexanes; elem. anal.;
DOI:10.1021/ic200010q