C₁₀H₈Br₂F₂

Base Information

• Chemical Name: C₁₀H₈Br₂F₂
• CAS No.: 1607805-21-9
• Molecular Formula: C₁₀H₈Br₂F₂
• Molecular Weight: 325.978
• Mol file: 1607805-21-9.mol

Synonyms:C₁₀H₈Br₂F₂

Chemical Property of C₁₀H₈Br₂F₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₈Br₂F₂

There total 3 articles about C₁₀H₈Br₂F₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H9BrF2O (2098118-22-8) → C10H8Br2F2 (1607805-21-9)

Guidance literature:

With pyridine; carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol500803r

Reference yield:

4-bromocinnamyl acetate (204326-54-5) → C10H8Br2F2 (1607805-21-9)

Guidance literature:

Multi-step reaction with 3 steps

1: diethylene glycol dimethyl ether / 0.5 h / 20 - 180 °C / Inert atmosphere

2: potassium carbonate / methanol / 12 h / 20 °C / Inert atmosphere

3: pyridine; triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; carbon tetrabromide; potassium carbonate; triphenylphosphine; In methanol; dichloromethane; diethylene glycol dimethyl ether;

DOI:10.1021/ol500803r

Reference yield:

C12H11BrF2O2 → C10H8Br2F2 (1607805-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 12 h / 20 °C / Inert atmosphere

2: pyridine; triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; carbon tetrabromide; potassium carbonate; triphenylphosphine; In methanol; dichloromethane;

DOI:10.1021/ol500803r

upstream raw materials:

C₁₀H₉BrF₂O

4-bromocinnamyl acetate

Downstream raw materials:

C₁₃H₁₃BrF₂