2,4-dichloro-1-deuterobenzene

Base Information

• Chemical Name: 2,4-dichloro-1-deuterobenzene
• CAS No.: 1044276-42-7
• Molecular Formula: C₆H₄Cl₂
• Molecular Weight: 147.996
• Mol file: 1044276-42-7.mol

Synonyms:2,4-dichloro-1-deuterobenzene

Chemical Property of 2,4-dichloro-1-deuterobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dichloro-1-deuterobenzene

There total 3 articles about 2,4-dichloro-1-deuterobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(2,4-dichlorophenyl)hydrazine (13123-92-7) → 2,4-dichloro-1-deuterobenzene (1044276-42-7)

Guidance literature:

With ammonium cerium (IV) nitrate; d⁽⁴⁾-methanol; at 20 ℃;

DOI:10.1055/s-2007-1072749

Reference yield: 80.0%

acetic acid-[N'-(2,4-dichloro-phenyl)-hydrazide] (14580-40-6) → 2,4-dichloro-1-deuterobenzene (1044276-42-7)

Guidance literature:

With ammonium cerium (IV) nitrate; d⁽⁴⁾-methanol; at 20 ℃;

DOI:10.1055/s-2007-1072749

Reference yield:

2,4 dichlorobenzoic acid (50-84-0) → 2,4-dichloro-1-deuterobenzene (1044276-42-7)

Guidance literature:

With water-d2; potassium hydroxide; In N,N-dimethyl-formamide; at 110 ℃; for 24h; chemoselective reaction; Schlenk technique;

DOI:10.1039/d1gc00924a

upstream raw materials:

acetic acid-[N'-(2,4-dichloro-phenyl)-hydrazide]

(2,4-dichlorophenyl)hydrazine

2,4 dichlorobenzoic acid