4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

Base Information

Chemical Name:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate
CAS No.:1616628-13-7
Molecular Formula:C₃₈H₃₁F₁₇O₉
Molecular Weight:954.632
Hs Code.:

Synonyms:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

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Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

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Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

There total 2 articles about 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₂₆O₉

: 200112-75-0
3-(perfluorooctyl)propyl iodide

: 1616628-13-7
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 3h;
DOI:10.1016/j.carres.2014.05.007

Reference yield:

: 428865-77-4
4-methoxyphenyl 2-O-benzyol-3-O-benzyl-β-D-glucopyranoside

: 1616628-13-7
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; potassium bromide; calcium hypochlorite; sodium hydrogencarbonate / dichloromethane; water / 0.75 h / 0 °C

2: N,N-dimethyl-formamide / 3 h / 60 °C

With calcium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; sodium hydrogencarbonate; potassium bromide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2014.05.007

Reference yield:

: O-(4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-α,β-D-glucopyranosyl)trichloroacetimidate

: 1616628-13-7
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

: 1616628-14-8
C₆₀H₅₅Cl₃F₁₇NO₁₇

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2014.05.007