N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

Base Information

Chemical Name:N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide
CAS No.:885431-00-5
Molecular Formula:C₂₀H₂₉NO₂S
Molecular Weight:347.522
Hs Code.:

Synonyms:N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

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Technology Process of N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

There total 1 articles about N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 17768-41-1
adamantylmethylamine

: 885431-00-5
N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

Guidance literature:: With sodium hydroxide; In chloroform; water; at 0 - 20 ℃; for 2h;

Reference yield: 99.0%

: 110-52-1
1,4-dibromo-butane

: 885431-00-5
N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

: 1059675-25-0
N-adamantan-1-ylmethyl-N-(4-bromo-butyl)-mesitylene-2-sulfonamide

Guidance literature:: 1,4-dibromo-butane; N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.333333h;

With sodium iodide; In N,N-dimethyl-formamide; mineral oil; at 75 ℃; for 2h;

Reference yield: 99.0%

: 885431-00-5
N-(((3r,5r,7r)-adamantan-1-yl)methyl)-2,4,6-trimethylbenzenesulfonamide

: 501-65-5
diphenyl acetylene

: N-((E)-1-((3r,5r,7r)-adamantan-1-yl)-2,3-diphenylallyl)-2,4,6-trimethylbenzenesulfonamide

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; dicyclohexylphenylphosphine; In 1,4-dioxane; at 120 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.1c00622