1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol

Base Information

• Chemical Name: 1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol
• CAS No.: 134753-59-6
• Molecular Formula: C₂₃H₃₅NO₂
• Molecular Weight: 357.536

Synonyms:1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol

Chemical Property of 1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol

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Technology Process of 1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol

There total 2 articles about 1-(tricyclo<3.3.1.1^3,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acide 5-(tricyclo<3.3.1.13,7>dec-1-yl)-tetrahydro-2-oxo-5-phenylfurane-3-carboxylique (134753-57-4) → 1-(tricyclo<3.3.1.13,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol (134753-59-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 36percent aq. CH₂O, Me₂NH / ethanol / 30 h / 0 °C

2: LiAlH₄ / tetrahydrofuran / 5 h / Heating

With lithium aluminium tetrahydride; formaldehyd; dimethyl amine; In tetrahydrofuran; ethanol;

DOI:10.1016/0223-5234(91)90213-7

Reference yield:

5-(tricyclo<3.3.1.13,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one (777821-90-6) → 1-(tricyclo<3.3.1.13,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol (134753-59-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Yield given; Heating;

DOI:10.1016/0223-5234(91)90213-7

Reference yield: 58.0%

1-(tricyclo<3.3.1.13,7>dec-1-yl)-3-(dimethylaminomethyl)-1-phenylbutane-1,4-diol (134753-59-6) → 5-(tricyclo<3.3.1.13,7>dec-1-yl)-tetrahydro-N,N-dimethyl-5-phenyl-3-furanemethanamine

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 5h; Heating;

DOI:10.1016/0223-5234(91)90213-7

upstream raw materials:

5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-dihydro-3-(dimethylaminomethyl)-5-phenylfuran-2(3H)-one

acide 5-(tricyclo<3.3.1.1^3,7>dec-1-yl)-tetrahydro-2-oxo-5-phenylfurane-3-carboxylique

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